2BHV
Structure of ComB10 of the Com Type IV secretion system of Helicobacter pylori
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-03-01 |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 69.735, 139.411, 168.442 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 3.000 |
R-factor | 0.259 |
Rwork | 0.257 |
R-free | 0.29300 |
Structure solution method | OTHER |
RMSD bond length | 0.015 |
RMSD bond angle | 1.274 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHARP |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 3.160 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.090 | 0.610 |
Number of reflections | 32829 | |
<I/σ(I)> | 11 | 2.3 |
Completeness [%] | 97.4 | 98 |
Redundancy | 3.7 | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | 8-14% (W/V) POLYETHYLENE GLYCOL (PEG) 8000, 100MM SODIUM CACODYLATE PH6.0 AND 200 MM MAGNESIUM ACETATE, pH 6.00 |