2BAP
Crystal structure of the N-terminal mDia1 Armadillo Repeat Region and Dimerisation Domain in complex with the mDia1 autoregulatory domain (DAD)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-05-28 |
Detector | MARRESEARCH |
Wavelength(s) | 0.95 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 138.450, 138.450, 210.890 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.980 - 3.300 |
R-factor | 0.292 |
Rwork | 0.288 |
R-free | 0.36400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1z2c |
RMSD bond length | 0.010 |
RMSD bond angle | 1.248 |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 3.400 |
High resolution limit [Å] | 3.300 | 3.300 |
Rmerge | 0.141 | |
Number of reflections | 18490 | 0 |
<I/σ(I)> | 16.79 | |
Completeness [%] | 81.9 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.1 | 293 | 3.7 M NaFormiate pH 7.1, 100 mM HEPES pH 7.1, 4% (w/v) PEG5000-MME, VAPOR DIFFUSION, HANGING DROP, temperature 293K |