2AZN

X-RAY Structure of 2,5-diamino-6-ribosylamino-4(3h)-pyrimidinone 5-phosphate reductase

Experimental procedure

Experimental method	MAD
Source type	SYNCHROTRON
Source details	MPG/DESY, HAMBURG BEAMLINE BW6
Synchrotron site	MPG/DESY, HAMBURG
Beamline	BW6
Detector technology	CCD
Detector	MARRESEARCH
Wavelength(s)	1.006, 1.009, 0.95
Spacegroup name	P 43 21 2
Unit cell lengths	137.171, 137.171, 213.870
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.000 - 2.700
R-factor	0.23
Rwork	0.230
R-free	0.25300
Structure solution method	MAD
Refinement software	CNS

Data quality characteristics

	Overall
Low resolution limit [Å]	25.000
High resolution limit [Å]	2.500
Number of reflections	134041

Crystallization Conditions

crystal ID	method	pH	temperature	details
1