2AJI
Crystal structure of the editing domain of E. coli leucyl-tRNA synthetase complexes with isoleucine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 123 |
Detector technology | IMAGE PLATE |
Collection date | 2005-01-01 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 112.487, 112.487, 135.023 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 3.200 |
R-factor | 0.23436 |
Rwork | 0.232 |
R-free | 0.28360 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.170 |
Phasing software | CNS |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.370 |
High resolution limit [Å] | 3.200 | 3.200 |
Rmerge | 0.091 | 0.410 |
Number of reflections | 7726 | |
<I/σ(I)> | 8.7 | 2.1 |
Completeness [%] | 89.4 | 89.4 |
Redundancy | 4.4 | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 9 | 293 | (NH4)2SO4, pH 9, VAPOR DIFFUSION, HANGING DROP, temperature 293K |