2A5X
Crystal Structure of a Cross-linked Actin Dimer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.2 |
Synchrotron site | ALS |
Beamline | 8.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-04-17 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.1 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 207.377, 54.372, 36.200 |
Unit cell angles | 90.00, 98.62, 90.00 |
Refinement procedure
Resolution | 90.000 - 2.490 |
R-factor | 0.19707 |
Rwork | 0.194 |
R-free | 0.25011 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1qz5 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.524 |
Data scaling software | SCALEPACK |
Phasing software | EPMR |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 90.000 | 2.590 |
High resolution limit [Å] | 2.490 | 2.490 |
Number of reflections | 13943 | |
<I/σ(I)> | 19.4 | 8.7 |
Completeness [%] | 99.6 | 99 |
Redundancy | 6.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.7 | 293 | 35% MPD, 100 mM sodium acetate pH 4.7, 20 mM calcium chloride, non-detergent sulfo-betaine, VAPOR DIFFUSION, HANGING DROP, temperature 293K |