278D
SUBSTITUTIONS AT C2' OF DAUNOSAMINE IN THE ANTICANCER DAUNORUBICIN ALTER ITS DNA-BINDING SEQUENCE SPECIFICITY
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 293 |
Detector technology | IMAGE PLATE |
Collection date | 1995-08-06 |
Detector | RIGAKU RAXIS IIC |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 28.250, 28.250, 53.670 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.800 |
R-factor | 0.183 |
RMSD bond length | 0.019 |
Data reduction software | MSC |
Refinement software | NUCLSQ |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 8.000 * | |
High resolution limit [Å] | 1.800 * | 1.800 * |
Rmerge | 0.060 | |
Completeness [%] | 83.8 * | |
Redundancy | 4.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6 | 298 | pH 6.00, VAPOR DIFFUSION, temperature 298.00K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | MPD | ||
3 | 1 | 1 | BACL2 | ||
4 | 1 | 1 | NA CACODYLATE | ||
5 | 1 | 1 | SPERMINE | ||
6 | 1 | 2 | WATER | ||
7 | 1 | 2 | MPD |