26LM

Crystal structure of cblb

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL02U1
Synchrotron site	SSRF
Beamline	BL02U1
Temperature [K]	273
Detector technology	PIXEL
Collection date	2023-07-03
Detector	DECTRIS EIGER2 S 9M
Wavelength(s)	0.979183
Spacegroup name	P 41 21 2
Unit cell lengths	71.840, 71.840, 212.311
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	50.420 - 1.950
R-factor	0.213
Rwork	0.212
R-free	0.23960
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.009
RMSD bond angle	1.168
Data scaling software	Aimless
Refinement software	PHENIX ((1.19.2_4158: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.800	1.900
High resolution limit [Å]	1.810	1.810
Rmerge	0.091	0.084
Rmeas	0.093	2.501
Rpim	0.018	0.551
Number of reflections	77285	2353
<I/σ(I)>	28
Completeness [%]	95.8
Redundancy	20	15
CC(1/2)	0.999	0.591

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	0.1 M Sodium chloride, 0.1 M BICINE pH 9.0, -20% v/v Polyethylene glycol monomethylether 550