266D
STRUCTURAL STUDIES ON NUCLEIC ACIDS
Experimental procedure
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 277 |
| Detector technology | IMAGE PLATE |
| Collection date | 1994-03-22 |
| Detector | RIGAKU RAXIS IIC |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 25.394, 40.837, 65.864 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | ? - 2.030 |
| R-factor | 0.166 |
| Structure solution method | MIR |
| RMSD bond length | 0.027 |
| RMSD bond angle | 0.064 |
| Data reduction software | RIGAKU |
| Data scaling software | RIGAKU |
| Refinement software | NUCLSQ |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 40.800 |
| High resolution limit [Å] | 2.030 |
| Rmerge | 0.068 |
| Number of reflections | 12395 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.1 | pH 7.10 |
Crystallization Reagents
| ID | crystal ID | solution ID | reagent name | concentration | details |
| 1 | 1 | 1 | WATER | ||
| 2 | 1 | 1 | NA CACODYLATE |
