260D
CRYSTAL STRUCTURE OF THE SELF-COMPLEMENTARY 5'-PURINE START DECAMER D(GCACGCGTGC) IN THE A-DNA CONFORMATION-PART II
Experimental procedure
Source type | ROTATING ANODE |
Source details | MACSCIENCE |
Detector technology | AREA DETECTOR |
Collection date | 1994-12-06 |
Detector | SIEMENS-NICOLET |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 38.970, 38.970, 77.340 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 8.000 - 1.900 |
R-factor | 0.186 |
Rwork | 0.186 |
RMSD bond length | 0.013 |
RMSD bond angle | 32.900 * |
Data reduction software | XENGEN (V. 2.0) |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 8.000 |
High resolution limit [Å] | 1.900 |
Rmerge | 0.031 |
Total number of observations | 9346 * |
Number of reflections | 2634 |
Completeness [%] | 91.0 |
Redundancy | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7 | pH 7.00, VAPOR DIFFUSION |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | MPD | ||
3 | 1 | 1 | NA CACODYLATE | ||
4 | 1 | 1 | [CO(NH3)6]3+ | ||
5 | 1 | 2 | WATER | ||
6 | 1 | 2 | MPD |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | DNA dodecamer | 1 (mM) | |
2 | 1 | drop | sodium cacodylate | 40 (mM) | |
3 | 1 | drop | cobalt hexamine | 0.5 (mM) | |
4 | 1 | reservoir | MPD | 45 (%) |