242D
MAD PHASING STRATEGIES EXPLORED WITH A BROMINATED OLIGONUCLEOTIDE CRYSTAL AT 1.65 A RESOLUTION.
Experimental procedure
| Source type | SYNCHROTRON |
| Source details | SRS BEAMLINE PX9.5 |
| Synchrotron site | SRS |
| Beamline | PX9.5 |
| Detector technology | IMAGE PLATE |
| Collection date | 1993-09-15 |
| Detector | MARRESEARCH |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 17.970, 30.980, 44.850 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 - 1.650 |
| R-factor | 0.17 |
| Structure solution method | MAD |
| RMSD bond length | 0.010 * |
| RMSD bond angle | 0.015 * |
| Data reduction software | DENZO |
| Data scaling software | CCP4 |
| Phasing software | MLPHARE |
| Refinement software | NUCLSQ |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * |
