Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL10U2 |
| Synchrotron site | SSRF |
| Beamline | BL10U2 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2025-12-23 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.979183 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 82.799, 83.959, 103.397 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 23.190 - 1.910 |
| R-factor | 0.1982 |
| Rwork | 0.197 |
| R-free | 0.22880 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.908 |
| Data reduction software | autoPX |
| Phasing software | PHASER |
| Refinement software | PHENIX (("2.0_5936": ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.960 |
| High resolution limit [Å] | 1.910 | 1.910 |
| Rmerge | 0.058 | 0.973 |
| Rmeas | 0.061 | 1.062 |
| Rpim | 0.018 | 0.411 |
| Number of reflections | 55088 | 3248 |
| <I/σ(I)> | 41.51 | 1.86 |
| Completeness [%] | 97.6 | 79.8 |
| Redundancy | 10.62 | 6.59 |
| CC(1/2) | 0.999 | 0.453 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6 | 289.15 | 1 mM MES 6.0, 8% PEG3350 |
