221D
INFLUENCE OF COUNTER-IONS ON THE CRYSTAL STRUCTURES OF DNA DECAMERS: BINDING OF [CO(NH3)6]3+ AND BA2+ TO A-DNA
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS IIC |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 24.726, 45.135, 47.515 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | ? - 1.900 |
R-factor | 0.2 |
RMSD bond length | 0.017 |
Refinement software | NUCLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.900 |
Rmerge | 0.053 * |
Number of reflections | 3156 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 6.5 | pH 6.50, VAPOR DIFFUSION |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | MPD | ||
3 | 1 | 1 | NA CACODYLATE | ||
4 | 1 | 1 | SPERMINE | ||
5 | 1 | 3 | WATER | ||
6 | 1 | 3 | SPERMINE |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | DNA duplex | 4 (mM) | 0.0025 ml | |
2 | 1 | sodium cacodylate | 50 (mM) | 0.01 ml | |
3 | 1 | MPD | 20 (%) | 0.0025 ml | |
4 | 1 | spermine | 10 (mM) | 0.0025 ml |