21FT

GABA aminotransferase from Arabidopsis thaliana

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL44XU
Synchrotron site	SPring-8
Beamline	BL44XU
Temperature [K]	100
Detector technology	PIXEL
Collection date	2025-11-05
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.899995
Spacegroup name	P 1
Unit cell lengths	62.178, 78.268, 93.216
Unit cell angles	96.76, 88.88, 106.11

Refinement procedure

Resolution	41.580 - 2.000
R-factor	0.1553
Rwork	0.153
R-free	0.19840
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	HKL-2000
Data scaling software	XDS
Phasing software	REFMAC
Refinement software	PHENIX (1.21_5207: ???)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.120
High resolution limit [Å]	2.000	2.000
Number of reflections	110288	17782
<I/σ(I)>	10.79
Completeness [%]	96.8
Redundancy	3.56
CC(1/2)	0.991	0.922

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	PEG 3350, Calcium acetate