1ZXA
Solution Structure of the Coiled-Coil Domain of cGMP-dependent Protein Kinase Ia
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | AVANCE | 500 | |
| 2 | Bruker | DMX | 600 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | TROSY version of HNCA, HNCACB, HNCACO |
| 2 | 1 | 1 | 2D 1H-15N Spin Echo Difference Experiments for 3-bond Jcc and Jnc measurement |
| 3 | 1 | 1 | Standard HNCO-based 3D experiments for measuring one-bond J(NH), J(NC'), and J(C'Ca) |
| 4 | 2 | 2 | Standard HNCO-based 3D experiments for measuring one-bond D(NH), D(NC'), and D(C'Ca) |
| 5 | 1 | 1 | Standard 2D experiments for measuring 15N T1 and T2 |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 7 | ambient | 303 |
| 2 | 7 | ambient | 303 |
Conformers
| Conformers Calculated Total Number | 20 |
| Conformers Submitted Total Number | 20 |
