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1ZWW

Crystal structure of endophilin-A1 BAR domain

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE BM14
Synchrotron siteESRF
BeamlineBM14
Temperature [K]100
Collection date2005-03-14
Spacegroup nameC 2 2 21
Unit cell lengths40.705, 121.651, 244.026
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution20.000 - 2.300
R-factor0.251
Rwork0.249
R-free0.28700
Structure solution methodSAD
RMSD bond length0.016
RMSD bond angle1.499
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareSOLVE
Refinement softwareREFMAC (5.2.0005)
Data quality characteristics
 Overall
Low resolution limit [Å]48.700
High resolution limit [Å]2.300
Number of reflections27463
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP9298sodium acetate, cadmium sulfate, VAPOR DIFFUSION, HANGING DROP, temperature 298K, pH 9.00

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