Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | BSRF BEAMLINE 3W1A |
| Synchrotron site | BSRF |
| Beamline | 3W1A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-10-09 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.9000, 0.9798, 0.9800 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 54.017, 57.546, 87.318 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 30.000 - 1.700 |
| R-factor | 0.208 |
| Rwork | 0.208 |
| R-free | 0.24100 |
| Structure solution method | MAD |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.520 |
| Data reduction software | AUTOMAR |
| Phasing software | SOLVE |
| Refinement software | CNS (1.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 1.770 |
| High resolution limit [Å] | 1.700 | 1.700 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 291 | PEG4000, Hepes, pH 8.50, VAPOR DIFFUSION, HANGING DROP, temperature 291K |
