1ZRT
Rhodobacter capsulatus cytochrome bc1 complex with stigmatellin bound
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL7-1 |
Synchrotron site | SSRL |
Beamline | BL7-1 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2001-03-14 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.0800 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 95.633, 154.360, 103.057 |
Unit cell angles | 90.00, 113.57, 90.00 |
Refinement procedure
Resolution | 59.770 - 3.510 |
R-factor | 0.224 |
Rwork | 0.221 |
R-free | 0.28870 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2bcc |
RMSD bond length | 0.019 |
RMSD bond angle | 2.187 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | PHENIX (dev_3885) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.000 | 3.630 |
High resolution limit [Å] | 3.500 | 3.500 |
Rmerge | 0.120 | 0.280 |
Number of reflections | 33596 | 3197 |
<I/σ(I)> | 8.5 | 3.9 |
Completeness [%] | 97.6 | 94 |
Redundancy | 2.68 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.2 | 277 | PEG-400, 0.1 M MgCl2, Heptanetriol, Cacodylate, Undecylmaltoside |
1 | VAPOR DIFFUSION, SITTING DROP | 5.2 | 277 | PEG-400, 0.1 M MgCl2, Heptanetriol, Cacodylate, Undecylmaltoside |
1 | VAPOR DIFFUSION, SITTING DROP | 5.2 | 277 | PEG-400, 0.1 M MgCl2, Heptanetriol, Cacodylate, Undecylmaltoside |