1ZOL
native beta-PGM
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2004-01-14 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 52.760, 57.190, 75.640 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 18.910 - 1.900 |
R-factor | 0.202 |
Rwork | 0.202 |
R-free | 0.21100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1lvh |
RMSD bond length | 0.011 |
RMSD bond angle | 1.500 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 18.910 | 2.020 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.038 | 0.137 |
Number of reflections | 18379 | |
<I/σ(I)> | 15.4 | 5.4 |
Completeness [%] | 98.6 | 96.7 |
Redundancy | 2.4 | 2.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 291 | 100 mM Tris HCl pH 8.5, 200 mM sodium acetate, 30% PEG 4000, VAPOR DIFFUSION, HANGING DROP, temperature 291K |