1ZOD

Crystal structure of dialkylglycine decarboxylase bound with cesium ion

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRL BEAMLINE BL9-1
Synchrotron site	SSRL
Beamline	BL9-1
Temperature [K]	100
Detector technology	CCD
Collection date	2004-04-15
Detector	SIEMENS
Wavelength(s)	0.98
Spacegroup name	P 64 2 2
Unit cell lengths	150.524, 150.524, 84.859
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	50.000 - 1.800
Rwork	0.200
R-free	0.22600
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1dka
RMSD bond length	0.016
RMSD bond angle	1.850
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	CNS
Refinement software	CNS

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	100.000	1.830
High resolution limit [Å]	1.800	1.800
Number of reflections	51040
Completeness [%]	96.7	96.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.4	298	PEG4K, MES, PLP, pH 6.4, VAPOR DIFFUSION, HANGING DROP, temperature 298K