1ZN2
Low Resolution Structure of Response Regulator StyR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE BW7B |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | BW7B |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2003-10-24 |
Detector | MARRESEARCH |
Wavelength(s) | 0.8416 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 41.660, 36.546, 75.120 |
Unit cell angles | 90.00, 100.32, 90.00 |
Refinement procedure
Resolution | 25.300 - 2.910 |
R-factor | 0.26871 |
Rwork | 0.265 |
R-free | 0.35232 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.410 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.300 | 2.950 |
High resolution limit [Å] | 2.910 | 2.910 |
Number of reflections | 4795 | |
Completeness [%] | 96.8 | 47.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.3 | 277 | PEG 4000, MgCl2, pH 8.3, VAPOR DIFFUSION, HANGING DROP, temperature 277K |