1ZKZ
Crystal Structure of BMP9
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-05-21 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0000 |
Spacegroup name | I 41 2 2 |
Unit cell lengths | 71.234, 71.234, 144.897 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 23.800 - 2.330 |
R-factor | 0.23254 |
Rwork | 0.231 |
R-free | 0.27181 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3bmp |
RMSD bond length | 0.017 |
RMSD bond angle | 1.866 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 23.800 | 50.000 | 2.400 |
High resolution limit [Å] | 2.320 | 5.000 | 2.320 |
Rmerge | 0.077 | 0.045 | 0.357 |
Number of reflections | 8142 | ||
Redundancy | 13.5 | 12.6 | 11.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 296 | 1-1.2 M Sodium Chloride, 7-10 mM Hexadecyltrimethylammonium Bromide 10 mM Magnesium Chloride, pH 7.5, temperature 296K, VAPOR DIFFUSION, HANGING DROP |