Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

1ZKY

Human Estrogen Receptor Alpha Ligand-Binding Domain In Complex With OBCP-3M and A Glucocorticoid Receptor Interacting Protein 1 Nr Box II Peptide

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 19-BM
Synchrotron siteAPS
Beamline19-BM
Temperature [K]77
Detector technologyCCD
Collection date2005-04-07
DetectorSBC-3
Wavelength(s)0.979
Spacegroup nameP 1 21 1
Unit cell lengths55.929, 84.129, 58.220
Unit cell angles90.00, 109.06, 90.00
Refinement procedure
Resolution27.010 - 2.250
R-factor0.18756
Rwork0.185
R-free0.23141
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1l2i
RMSD bond length0.011
RMSD bond angle1.171
Data reduction softwareHKL-2000
Data scaling softwareSCALEPACK
Refinement softwareREFMAC (5.2.0005)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]55.0482.330
High resolution limit [Å]2.2502.250
Rmerge0.1180.564
Number of reflections24141
<I/σ(I)>10.7592
Completeness [%]59.7
Redundancy2.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP72890.2M sodium malonate, 20% PEG 3350, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 289K

227111

PDB entries from 2024-11-06

PDB statisticsPDBj update infoContact PDBjnumon