1ZIQ
Deuterated gammaE crystallin in D2O solvent
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-03-11 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.9393 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 37.390, 43.330, 101.530 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.630 - 1.720 |
R-factor | 0.19 |
Rwork | 0.185 |
R-free | 0.22500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1a5d |
RMSD bond length | 0.018 |
RMSD bond angle | 1.761 |
Data reduction software | MOSFLM |
Data scaling software | XDS |
Phasing software | MOLREP |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.630 | 1.850 |
High resolution limit [Å] | 1.720 | 1.720 |
Number of reflections | 18328 | |
Completeness [%] | 99.2 | 89.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 293 | PEG 3350, Magnesium Acetate, D2O, pH 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 293K |