1ZIM

GCN4-LEUCINE ZIPPER CORE MUTANT ASN16GLN IN THE TRIMERIC STATE

Experimental procedure

Source type	SEALED TUBE
Detector technology	IMAGE PLATE
Collection date	1994-05
Detector	RIGAKU RAXIS
Spacegroup name	P 21 21 21
Unit cell lengths	36.240, 46.610, 50.830
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 - 2.000
R-factor	0.178 *
Rwork	0.178
RMSD bond length	0.013
RMSD bond angle	2.300
Data reduction software	R-AXIS
Refinement software	TNT

Data quality characteristics

	Overall
Low resolution limit [Å]	6.000 *
High resolution limit [Å]	2.000 *
Rmerge	0.077
Total number of observations	12314 *
Number of reflections	5493
Completeness [%]	87.0
Redundancy	2.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *		24 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	peptide	20 (mM)
2	1	reservoir		50 (mM)
3	1	reservoir		0.4 (M)
4	1	reservoir	PEG1450	2.5 (%)