1ZIJ

GCN4-LEUCINE ZIPPER CORE MUTANT ASN16ABA IN THE TRIMERIC STATE

Experimental procedure

Source type	SEALED TUBE
Detector technology	IMAGE PLATE
Collection date	1994-08
Detector	RIGAKU RAXIS
Spacegroup name	P 21 21 21
Unit cell lengths	37.190, 46.590, 51.530
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 - 2.000
R-factor	0.184 *
Rwork	0.184
RMSD bond length	0.010
RMSD bond angle	1.900
Data reduction software	R-AXIS
Data scaling software	R-AXIS
Refinement software	TNT

Data quality characteristics

	Overall
High resolution limit [Å]	2.000 *
Rmerge	0.046
Total number of observations	18908 *
Number of reflections	5954
Completeness [%]	85.0
Redundancy	3.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, sitting drop *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	peptide	20 (mg/ml)
2	1	reservoir	HEPES	0.1 (M)
3	1	reservoir	sodium citrate	1.0 (M)