1ZIB
REDUCED PSEUDOAZURIN
Experimental procedure
| Detector technology | IMAGE PLATE |
| Collection date | 1995-10-13 |
| Detector | RIGAKU RAXIS IIC |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 56.650, 61.670, 30.420 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 10.000 - 2.000 |
| R-factor | 0.1687 * |
| Rwork | 0.169 |
| RMSD bond length | 0.018 |
| RMSD bond angle | 0.039 |
| Data reduction software | PROCESS |
| Refinement software | PROLSQ |
Data quality characteristics
| Overall | |
| Rmerge | 0.037 |
| Number of reflections | 7257 |
| Completeness [%] | 96.3 |
| Redundancy | 3.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 6 * | 4 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | protein | 10 (mg/ml) | |
| 2 | 1 | drop | sodium cacodylate | 0.1 (M) | |
| 3 | 1 | drop | sodium azide | 1 (mM) | |
| 4 | 1 | drop | ammonium sulfate | 50 (%sat) | |
| 5 | 1 | reservoir | sodium cacodylate | 0.1 (M) | |
| 6 | 1 | reservoir | sodium azide | 1 (mM) | |
| 7 | 1 | reservoir | PEG8000 | 5 (%(w/v)) | |
| 8 | 1 | reservoir | ammonium sulfate | 70 (%sat) |
