1ZDI
RNA BACTERIOPHAGE MS2 COAT PROTEIN/RNA COMPLEX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX9.6 |
Synchrotron site | SRS |
Beamline | PX9.6 |
Detector technology | IMAGE PLATE |
Detector | MARRESEARCH |
Spacegroup name | H 3 2 |
Unit cell lengths | 288.000, 288.000, 653.000 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 10.000 - 2.700 |
R-factor | 0.202 * |
Rwork | 0.202 |
RMSD bond length | 0.016 * |
RMSD bond angle | 2.070 * |
Data reduction software | DENZO |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 8.100 * | |
High resolution limit [Å] | 2.700 * | 2.700 * |
Rmerge | 0.092 | 0.186 * |
Number of reflections | 193997 | |
Completeness [%] | 75.3 * | 51.4 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 * | VAPOR DIFFUSION, HANGING DROP |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | PEG 8000 | ||
3 | 1 | 1 | NA PHOSPHATE | ||
4 | 1 | 1 | NA AZIDE | ||
5 | 1 | 2 | WATER | ||
6 | 1 | 2 | NA PHOSPHATE | ||
7 | 1 | 2 | NA AZIDE |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | capsid | 0.6 (mg/ml) | |
2 | 1 | drop | PEG8000 | 1.25 (%(w/v)) | |
3 | 1 | drop | sodium phosphate | 0.1 (M) | |
4 | 1 | drop | sodium azide | 0.02 (%(w/v)) | |
5 | 1 | reservoir | sodium phosphate | 0.4 (M) | |
6 | 1 | reservoir | sodium azide | 0.02 (%(w/v)) |