1ZA5
Q69H-FeSOD
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 100 |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 41.202, 84.921, 61.634 |
| Unit cell angles | 90.00, 108.37, 90.00 |
Refinement procedure
| Resolution | 19.960 - 1.800 |
| R-factor | 0.199 |
| Rwork | 0.199 |
| R-free | 0.23700 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.700 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | CNS |
| Refinement software | CNS (1.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 1.880 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Number of reflections | 32845 | |
| Completeness [%] | 88.0 | 43 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8.66 | 277 | MgCl2, PEG8000, pH 8.66, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
