1Z7S

The crystal structure of coxsackievirus A21

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 14-BM-C
Synchrotron site	APS
Beamline	14-BM-C
Temperature [K]	100
Detector technology	CCD
Collection date	2000-01-01
Detector	ADSC QUANTUM 4
Wavelength(s)	1.00
Spacegroup name	P 42 3 2
Unit cell lengths	348.014, 348.014, 348.014
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	49.720 - 3.200
R-factor	0.224
Rwork	0.224
R-free	0.23500
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	1.400
Data reduction software	DENZO
Phasing software	SnB (OF DPS SUITE)
Refinement software	CNS (1.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	3.310
High resolution limit [Å]	3.200	3.200
Rmerge	0.119	0.238
Number of reflections	106927
Completeness [%]	97.1	88.9
Redundancy	17	11

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	6.4	277	sodium chloride, citrate, glycerol, pH 6.4, VAPOR DIFFUSION, SITTING DROP, temperature 277K