1Z6I
Crystal structure of the ectodomain of Drosophila transmembrane receptor PGRP-LCa
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-5A |
Synchrotron site | Photon Factory |
Beamline | BL-5A |
Temperature [K] | 110 |
Detector technology | CCD |
Collection date | 2005-01-22 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0000 |
Spacegroup name | P 41 3 2 |
Unit cell lengths | 105.799, 105.799, 105.799 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 74.540 - 2.500 |
R-factor | 0.215 |
Rwork | 0.213 |
R-free | 0.24100 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.268 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 74.540 | 2.590 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.062 | 0.558 |
Number of reflections | 7439 | |
<I/σ(I)> | 27.44 | 2.42 |
Completeness [%] | 99.4 | 99.6 |
Redundancy | 6.6 | 6.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.2 | 298 | ammonium sulphate, phosphate citrate, pH 4.2, VAPOR DIFFUSION, HANGING DROP, temperature 298K, temperature 298.0K |