1Z4A
Ferritin from T. maritima
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MPG/DESY, HAMBURG BEAMLINE BW6 |
Synchrotron site | MPG/DESY, HAMBURG |
Beamline | BW6 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-03-02 |
Detector | MARRESEARCH |
Wavelength(s) | 1.05 |
Spacegroup name | H 3 2 |
Unit cell lengths | 175.650, 175.650, 357.890 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 15.000 - 2.300 |
R-factor | 0.21 |
Rwork | 0.206 |
R-free | 0.24700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1bfr |
RMSD bond length | 0.011 |
RMSD bond angle | 1.170 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.000 | 2.420 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.082 | 0.349 |
Number of reflections | 92569 | |
<I/σ(I)> | 6.1 | 1.7 |
Completeness [%] | 98.5 | 98.5 |
Redundancy | 5.7 | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |