1Z3X
Structure of Gun4 from Thermosynechococcus elongatus
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | NSLS |
Synchrotron site | NSLS |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-02-04 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.976, 0.9802, 0.9660 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 58.295, 40.672, 62.372 |
Unit cell angles | 90.00, 115.40, 90.00 |
Refinement procedure
Resolution | 50.000 - 1.500 |
R-factor | 0.18042 |
Rwork | 0.179 |
R-free | 0.20856 |
Structure solution method | MAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.117 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0001) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.539 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.068 | 0.467 |
Number of reflections | 42482 | |
Completeness [%] | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 20% PEG 3350, 0.2 M NH3Cl, VAPOR DIFFUSION, SITTING DROP, temperature 277K |