1Z2X
Crystal structure of mouse Vps29
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 2003-08-16 |
Detector | MARRESEARCH |
Wavelength(s) | 1.541 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 55.912, 68.321, 60.166 |
Unit cell angles | 90.00, 106.98, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.220 |
R-factor | 0.17591 |
Rwork | 0.173 |
R-free | 0.22765 |
Structure solution method | MIR |
RMSD bond length | 0.019 |
RMSD bond angle | 1.829 |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | SHARP |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.300 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.069 | 0.216 |
Number of reflections | 21420 | |
<I/σ(I)> | 16.8 | 6.3 |
Completeness [%] | 99.4 | 99.4 |
Redundancy | 3.8 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 289 | 0.1M Tris, 0.2M NaCl, 20% PEG3000, pH 8.5, VAPOR DIFFUSION, SITTING DROP, temperature 289K |