1Z24

The molecular structure of insecticyanin from the tobacco hornworm Manduca sexta L. at 2.6 A resolution.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Temperature [K]	278
Detector technology	FILM
Collection date	1986-01-01
Detector	film
Spacegroup name	P 43 21 2
Unit cell lengths	115.400, 115.400, 71.500
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	50.000 - 2.600
Structure solution method	MIR
Data scaling software	A (PROGRAM BY M. ROSSMAN (ORIGINAL VERSION))
Phasing software	HEAVY

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.600
Number of reflections	14167
Completeness [%]	99.0

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	batch	5.5	293	20% PEG8000, 100 mM NaCl, 100 mM Nasuccinate, pH 5.5, batch, temperature 293K