1Z13
Crystal Structure of Bovine Low Molecular Weight PTPase Complexed with Molybdate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 1995-01-01 |
Detector | RIGAKU RAXIS II |
Wavelength(s) | 1.54 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 95.300, 43.400, 41.200 |
Unit cell angles | 90.00, 113.40, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.200 |
R-factor | 0.159 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1dg9 |
RMSD bond length | 0.010 |
RMSD bond angle | 2.450 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | TNT |
Refinement software | TNT |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.200 |
Number of reflections | 5798 |
Completeness [%] | 73.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 295 | PEG 4000, HEPES, Isopropanol, Na2MoO4, pH 7.5, VAPOR DIFFUSION, SITTING DROP, temperature 295K |