1Z0I
GDP-Bound Rab21 GTPase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2004-03-13 |
Detector | MAR scanner 300 mm plate |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 36.295, 88.861, 118.030 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 12.000 - 2.330 |
R-factor | 0.23162 |
Rwork | 0.229 |
R-free | 0.27844 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | Polyalanine Rab21 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.406 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.370 |
High resolution limit [Å] | 2.300 | 2.300 |
Number of reflections | 8301 | |
<I/σ(I)> | 17.4 | 4.3 |
Completeness [%] | 89.4 | 75.9 |
Redundancy | 2 | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 277 | 20% PEG 6000, 10% Glycerol, 200mM Na acetate, pH 4.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |