1YZR
Manganese peroxidase-Sm(III) complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 110 |
| Detector technology | IMAGE PLATE |
| Collection date | 1998-10-19 |
| Detector | RIGAKU RAXIS IV |
| Wavelength(s) | 1.5418 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 160.667, 45.293, 52.850 |
| Unit cell angles | 90.00, 97.12, 90.00 |
Refinement procedure
| Resolution | 8.000 - 1.600 |
| R-factor | 0.1537 |
| Rwork | 0.149 |
| R-free | 0.16340 |
| Structure solution method | FOURIER SYNTHESIS |
| Starting model (for MR) | 1yyd |
| RMSD bond length | 0.009 |
| RMSD bond angle | 0.023 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | SHELXL |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 161.000 | 1.670 |
| High resolution limit [Å] | 1.600 | 1.600 |
| Number of reflections | 48465 | |
| Completeness [%] | 98.0 | 80 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277 | PEG 8K, sodium cacodylate, ammonium sulfate, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
