1YYG
Manganese peroxidase complexed with Cd(II) inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 1998-04-15 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 160.352, 45.259, 52.714 |
Unit cell angles | 90.00, 97.21, 90.00 |
Refinement procedure
Resolution | 8.000 - 1.600 |
Rwork | 0.165 |
R-free | 0.22480 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 1yyd |
RMSD bond length | 0.009 |
RMSD bond angle | 0.023 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | SHELXL |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 8.000 | 1.630 |
High resolution limit [Å] | 1.600 | 1.600 |
Number of reflections | 47574 | |
<I/σ(I)> | 22 | |
Completeness [%] | 96.0 | 64 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277 | PEG 8K, sodium cacodylate, ammonium sulfate, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |