1YXT
Crystal Structure of Kinase Pim1 in complex with AMPPNP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-06-21 |
Detector | ADSC QUANTUM 4 |
Spacegroup name | P 65 |
Unit cell lengths | 95.566, 95.566, 80.862 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 81.650 - 2.000 |
R-factor | 0.183 |
Rwork | 0.181 |
R-free | 0.21600 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 1.568 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.1.25) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 82.760 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.057 | 0.715 |
Number of reflections | 28420 | |
<I/σ(I)> | 11.4 | 1 |
Completeness [%] | 99.9 | 100 |
Redundancy | 4.2 | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 277 | Na Acetate, Imidazole, pH 6.5, VAPOR DIFFUSION, SITTING DROP, temperature 277K |