1YXP
HIV-1 DIS RNA subtype F- Zn soaked
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 120 |
Detector technology | CCD |
Collection date | 2004-12-13 |
Detector | MARRESEARCH |
Wavelength(s) | 1.28238 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 27.275, 118.629, 93.334 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 7.980 - 2.400 |
R-factor | 0.27 |
Rwork | 0.270 |
R-free | 0.30300 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.006 |
RMSD bond angle | 1.000 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.550 |
High resolution limit [Å] | 2.400 | 2.400 |
Number of reflections | 10685 | |
<I/σ(I)> | 15.2 | 3.2 |
Completeness [%] | 94.4 | 97.5 |
Redundancy | 2.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 310 | PEG8000, Ammonium sulfate, MgCl2, Na Cacodylate, spermine, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 310K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | PEG8000 | ||
10 | 1 | 2 | Na Cacodylate | ||
2 | 1 | 1 | Ammonium sulfate | ||
3 | 1 | 1 | MgCl2 | ||
4 | 1 | 1 | Na Cacodylate | ||
5 | 1 | 1 | spermine | ||
6 | 1 | 1 | H2O | ||
7 | 1 | 2 | PEG8000 | ||
8 | 1 | 2 | Ammonium sulfate | ||
9 | 1 | 2 | MgCl2 |