1YXJ

Crystal structure of human lectin-like oxidized low-density lipoprotein receptor 1 (LOX-1) at low pH

Experimental procedure

Experimental method	MAD
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL40B2
Synchrotron site	SPring-8
Beamline	BL40B2
Temperature [K]	100
Detector technology	CCD
Collection date	2003-09-27
Detector	ADSC QUANTUM 4
Wavelength(s)	1.0
Spacegroup name	P 21 21 21
Unit cell lengths	62.636, 68.828, 79.133
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	28.180 - 1.780
R-factor	0.211
Rwork	0.211
R-free	0.23400
Structure solution method	MAD
RMSD bond length	0.005
RMSD bond angle	1.200
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	SHARP
Refinement software	CNS (0.9)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	1.780
Rmerge	0.053
Number of reflections	33424
Completeness [%]	99.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	3.6	293	Citrate, pH 3.6, VAPOR DIFFUSION, HANGING DROP, temperature 293K