1YWA
0.9 A Structure of NP4 from Rhodnius Prolixus complexed with CO at pH 5.6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 14-BM-C |
Synchrotron site | APS |
Beamline | 14-BM-C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-07-30 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.900 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 70.079, 42.587, 52.998 |
Unit cell angles | 90.00, 94.36, 90.00 |
Refinement procedure
Resolution | 10.000 - 0.890 |
R-factor | 0.121 |
Rwork | 0.120 |
R-free | 0.15000 |
Starting model (for MR) | PDB ID 1KOI |
RMSD bond length | 0.015 |
RMSD bond angle | 0.034 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.000 | 0.920 |
High resolution limit [Å] | 0.890 | 0.890 |
Number of reflections | 107559 | |
<I/σ(I)> | 26.9 | 3.6 |
Completeness [%] | 90.0 | 70 |
Redundancy | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 298 | 2.8 M ammonium phosphate, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 298K |