1YVD
GppNHp-Bound Rab22 GTPase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2003-01-01 |
Detector | MAR scanner 300 mm plate |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 45.536, 45.536, 150.338 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.930 |
R-factor | 0.19281 |
Rwork | 0.190 |
R-free | 0.25870 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | Rab3a polyalanine |
RMSD bond length | 0.009 |
RMSD bond angle | 1.111 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.960 |
High resolution limit [Å] | 1.905 | 1.900 |
Number of reflections | 13168 | |
<I/σ(I)> | 33.9 | 10.4 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 9 | 9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 277 | PEG6000, Lithium chloride, MES, Glycerol, pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 277K |