1YQT
RNase-L Inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-02-05 |
Detector | MARRESEARCH |
Wavelength(s) | 0.9790 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 59.680, 74.640, 123.690 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.000 - 1.900 |
R-factor | 0.199 |
Rwork | 0.199 |
R-free | 0.22500 |
Structure solution method | SAD |
RMSD bond length | 0.012 |
RMSD bond angle | 1.500 |
Data reduction software | TRUNCATE |
Data scaling software | CCP4 ((TRUNCATE)) |
Phasing software | SHARP |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.000 | 1.940 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 43582 | |
Completeness [%] | 95.2 | 72 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.8 | 298 | TRIS, EDTA, NaCl, NaCitrate, pH 7.8, VAPOR DIFFUSION, SITTING DROP, temperature 298K |