1YPU

Human Oxidized Low Density Lipoprotein Receptor LOX-1 C2 Space Group

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RUH3R
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2004-08-11
Detector	RIGAKU RAXIS IV
Spacegroup name	C 1 2 1
Unit cell lengths	71.300, 49.500, 76.700
Unit cell angles	90.00, 98.60, 90.00

Refinement procedure

Resolution	10.000 - 2.050
R-factor	0.183
Rwork	0.183
R-free	0.23800
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1mpu 1k9i 1q03
RMSD bond length	0.005
RMSD bond angle	1.300
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	MOLREP
Refinement software	CNS (1.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.120
High resolution limit [Å]	2.050	2.050
Number of reflections	16573
<I/σ(I)>	29	12
Completeness [%]	98.7	97.5
Redundancy	4.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		9	277	PEG10K, Bicine, Dioxane, HEPES, NaCl, pH 9.0, VAPOR DIFFUSION, HANGING DROP, temperature 277K