1YPQ
Human Oxidized Low Density Lipoprotein Receptor LOX-1 Dioxane Complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-04-12 |
Detector | MARMOSAIC 225 mm CCD |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 70.700, 49.100, 76.300 |
Unit cell angles | 90.00, 98.50, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.450 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.270 | |
Number of reflections | 50675 | |
<I/σ(I)> | 25 | 2.4 |
Completeness [%] | 99.0 | 91.8 |
Redundancy | 4.1 | 1.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 9 | 277 | PEG10K, Bicine, Dioxane, HEPES, NaCl, pH 9.0, VAPOR DIFFUSION, HANGING DROP, temperature 277K |