1YPP
ACID ANHYDRIDE HYDROLASE
Experimental procedure
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | X11 |
| Detector technology | IMAGE PLATE |
| Detector | MARRESEARCH |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 116.000, 106.200, 56.100 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 10.000 - 2.400 |
| R-factor | 0.19 * |
| RMSD bond length | 0.022 |
| RMSD bond angle | 0.031 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | PROLSQ |
Data quality characteristics
| Overall | Outer shell | |
| High resolution limit [Å] | 2.400 * | 2.400 * |
| Rmerge | 0.095 | 0.199 * |
| Number of reflections | 21721 * | |
| Completeness [%] | 79.0 * | 62 * |
| Redundancy | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 6.2 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | MES | 0.03 (M) | |
| 3 | 1 | 1 | phosphate | 0.5 (mM) | |
| 4 | 1 | 1 | MPD |
