1YPI

STRUCTURE OF YEAST TRIOSEPHOSPHATE ISOMERASE AT 1.9-ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	P 1 21 1
Unit cell lengths	61.150, 98.550, 49.260
Unit cell angles	90.00, 91.20, 90.00

Refinement procedure

Resolution	40.000 - 1.900
R-factor	0.21
RMSD bond length	0.025
RMSD bond angle	0.048
Refinement software	PROLSQ

Data quality characteristics

	Overall
Low resolution limit [Å]	3.000 *
High resolution limit [Å]	1.900 *
Rmerge	0.113 *
Number of reflections	2028 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	yeast triosephosphate isomerase	20 (mg/ml)
2	1	reservoir	ammonium sulfate	12 (%sat)
3	1	reservoir	EDTA	1 (mM)
4	1	reservoir	mercaptoethanol	1 (mM)
5	1	reservoir	Tris-HCl	50 (mM)
6	1	reservoir	PEG4000	16 (%)