1YP4
Crystal structure of potato tuber ADP-glucose pyrophosphorylase in complex with ADP-glucose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 32-ID |
Synchrotron site | APS |
Beamline | 32-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-11-01 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.99997 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 79.857, 137.964, 90.832 |
Unit cell angles | 90.00, 112.91, 90.00 |
Refinement procedure
Resolution | 19.990 - 2.300 |
R-factor | 0.183 |
Rwork | 0.183 |
R-free | 0.24400 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.007 |
RMSD bond angle | 1.400 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Number of reflections | 66734 | |
Completeness [%] | 99.7 | 99.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |