1YOY
Predicted coding region AF1432 from Archaeoglobus Fulgidus
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-BM |
| Synchrotron site | APS |
| Beamline | 19-BM |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-12-18 |
| Detector | CUSTOM-MADE |
| Wavelength(s) | 0.97945 |
| Spacegroup name | H 3 2 |
| Unit cell lengths | 131.799, 131.799, 58.178 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 19.460 - 2.000 |
| R-factor | 0.18611 |
| Rwork | 0.184 |
| R-free | 0.23589 |
| Structure solution method | SAD |
| RMSD bond length | 0.019 |
| RMSD bond angle | 1.630 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | SnB |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.070 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Number of reflections | 13058 | |
| Completeness [%] | 95.2 | 65.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.2 | 297 | 2.5M (NH4)2SO4, 0.1M t-Na citrate, pH 5.2, VAPOR DIFFUSION, HANGING DROP, temperature 297K |
